Introduction of a new synthetic route about Copper(I) bromide

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Copper(I) bromide, 7787-70-4

7787-70-4, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. Copper(I) bromide, cas is 7787-70-4,the copper-catalyst compound, it is a common compound, a new synthetic route is introduced below.

General procedure: The complexes were prepared according to the following method [14]: 1mmol of copper(I) bromide or copper(I) chloride is stirred in methanol until complete dissolution. Then, 2.1mmol of the corresponding phosphine ligand was added. The mixture was stirred at 60C for 30min. under nitrogen atmosphere. A microcrystalline precipitate was obtained by concentration of the solution at reduced pressure. The solid product was dissolved in a dichloromethane/methanol mixture and the solution was gradually cooled to 4C to give an air stable and colorless crystalline solid suitable for X-ray single-crystal diffraction studies.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Copper(I) bromide, 7787-70-4

Reference£º
Article; Espinoza, Sully; Arce, Pablo; San-Martin, Enrique; Lemus, Luis; Costamagna, Juan; Farias, Liliana; Rossi, Miriam; Caruso, Francesco; Guerrero, Juan; Polyhedron; vol. 85; (2014); p. 405 – 411;,
Copper catalysis in organic synthesis – NCBI
Special Issue “Fundamentals and Applications of Copper-Based Catalysts”